Kinetic determination of beryllium using decomposition of its complex with chlorophosphonazor
Автор: Danilina E.I., Akatieva Yu.V.
Журнал: Вестник Южно-Уральского государственного университета. Серия: Химия @vestnik-susu-chemistry
Рубрика: Аналитическая химия
Статья в выпуске: 1 т.6, 2014 года.
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Fast decomposition of beryllium complex with Chlorophosphonazo R in the absence of acetylacetone can be used for its kinetic determination by the tangent method. Analysis time drops from 30 min to 2 min. Optimal conditions and metrological characteristics of the procedure have been found. In the presence of EDTA selectivity, precision and sensitivity increase. The lower limit of concentration range is 0.15 mg/mL, the relative error does not exceed 2 %, while the observed errors of reproducibility are less than 3.3 %. Selectivity factors for a number of interfering cations and anions have been determined.
Kinetic analysis, tangent method, photometric analysis, beryllium, chloro-phosphonazo r
Короткий адрес: https://sciup.org/147160281
IDR: 147160281