Possibilities of application of methods of X-ray phase and X-ray diffraction analysis in the forensic science

Автор: Konstantin O. Smirnov, Vladimir V. Akatyev, Yulia A. Amelchenko

Журнал: НБИ технологии @nbi-technologies

Рубрика: Инновации в металлургии и материаловедении

Статья в выпуске: 3 т.15, 2021 года.

Бесплатный доступ

The paper reflects various aspects of the use of X-ray investigation methods, their advantages and application in forensic science of the phase composition of metals, paint and varnish coatings and paintwork materials, fragments of explosive devices. Practical examples of X-ray diffraction analysis application for thin film specimens made on the basis of paints containing alkyd varnish, pigments, fillers and solvents of various colour range have been examined. Influence of true physical broadening, on lines of diffractograms taken for samples exposed to shock wave action was also studied. It was found that this broadening is directly connected with influence of microstrains and fine dispersion of mosaic structure blocks. Based on the obtained X-ray diffraction analysis data, the dislocation density was calculated by three methods. Based on summarized experimental and literature data, the dependence of microstrains on the explosive weight was plotted, which can be used as a reference standard for comparison in expert studies of samples exposed to shock-wave impact

Еще

X-ray structural analysis, X-ray phase analysis, diffractogram, fine structure, mosaic blocks, microstrains, dislocation density

Короткий адрес: https://sciup.org/149138109

IDR: 149138109   |   DOI: 10.15688/NBIT.jvolsu.2021.3.6

Статья научная