Monitoring the presence of residues of lasalocid in feed samples HPLC-MS/MS
Автор: Rosa E. gavilN., Carolina neboT., Alejandra iglesiaS., Beatriz vazqueZ., Jose M. mirandA., Carlos M. francO., Alberto cepedA.
Журнал: Вестник Алматинского технологического университета @vestnik-atu
Рубрика: Естественные науки
Статья в выпуске: 4 (100), 2013 года.
Бесплатный доступ
Coccidiostats are veterinary medicine licensed to prevent and treat coccidiosis and histomoniasis. Due to the unavoidable carryover of these substances during the fabrication the European Commission decided to set up maxim level of coccidiostats in non-target feeds (Regulation 574/2011), including lasalocid. In this work an easy and cheap HPLC-MS/MS method for the analysis of lasalocid in medicated and contaminated feed is presented. The method only required 5 ml of acetonitrile and the detection is achieved for concentration between 60 and 1500 μg/Kg. The method full fills the criteria of the European Decision 2002/657/EC for the detection of lasalocid.
Feeds, lasalocid, hplc-ms/ms method
Короткий адрес: https://sciup.org/140205011
IDR: 140205011
Список литературы Monitoring the presence of residues of lasalocid in feed samples HPLC-MS/MS
- Galarini, R., Fioroni, L., Angelucci, F., Tovo, G. R., & Cristofani, E. (2009). Simultaneous determination of eleven quinolones in animal feed by liquid chromatography with fluorescence and ultraviolet absorbance detection. Journal of Chromatography A, 1216. -Р. 8158-8164.
- COMMISSION REGULATION (EU) No 574/2011 of 16 June 2011 amending Annex I to Directive 2002/32/EC of the European Parliament and of the Council as regards maximum levels for nitrite, melamine, Ambrosia spp. and carry-over of certain coccidiostats and histomonostats and consolidating Annexes I and II thereto L 159. -Р. 7-24.
- Focht, C. (2008). Determination of Lasalocid Sodium in Animal Feeds and Premixes by Reversed-Phase Liquid Chromatography: Collaborative Study. Journal of AOAC International, 91. -Р. 479-488.
- Vincent, U., Ezerskis, Z., Chedin, M., Von Holst, C. (2011). Determination of ionophore coccidiostats in feeding stuffs by liquid chromatography-tandem mass spectrometry. Part II. Application to cross-contamination levels and non-targeted feed. Journal of Pharmaceutical and Biomedical Analysis 54. -Р. 526-534.
- Mark Cronly, M., Behana, P., Foleya, B., Maloneb, E., Shearanb, P., Regan, L. (2011). Determination of eleven coccidiostats in animal feed by liquid chromatography-tandem mass spectrometry at cross contamination levels Analytica Chimica Acta 700. -Р. 26-33.
